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  • P-ISSN 2233-4203
  • E-ISSN 2093-8950

Validation of Bulk Analysis with Simulated Swipe Samples Containing Ultra-Trace Amounts of Uranium and Plutonium Using MC-ICP-MS

Mass Spectrometry Letters / Mass Spectrometry Letters, (P)2233-4203; (E)2093-8950
2015, v.6 no.3, pp.75-79
https://doi.org/10.5478/MSL.2015.6.3.75
Sang Ho Lim (Korea Atomic Energy Research Institute, University of Science and Technology)
Sun-Ho Han (Korea Atomic Energy Research Institute)
Jong-Ho Park (Korea Atomic Energy Research Institute, University of Science and Technology)
Ranhee Park (Korea Atomic Energy Research Institute)
Min Young Lee (Korea Atomic Energy Research Institute)
Jinkyu Park (Korea Atomic Energy Research Institute)
Chi-Gyu Lee (Korea Atomic Energy Research Institute)
Kyuseok Song (Korea Atomic Energy Research Institute)
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Abstract

Suitable analytical procedures for the bulk analysis of ultra-trace amounts of uranium and plutonium have been developed using multi-collector inductively coupled mass spectrometry (MC–ICP–MS). The quantification and determination of the isotopic ratios of uranium and plutonium in three simulated swipe samples, a swipe blank, and a process blank were per- formed to validate the analytical performance. The analytical results for the simulated swipe samples were in good agreement with the certified values, based on the measurement quality goals for the analysis of bulk environmental samples recommended by the International Atomic Energy Agency (IAEA)

keywords
Bulk analysis, Environmental samples, Chemical separation, IDMS, MC-ICP-MS


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투고일Submission Date
2015-08-21
수정일Revised Date
2015-09-04
게재확정일Accepted Date
2015-09-07
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Mass Spectrometry Letters