• P-ISSN2233-4203
  • E-ISSN2093-8950

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  • P-ISSN 2233-4203
  • E-ISSN 2093-8950

Validation of Bulk Analysis with Simulated Swipe Samples Containing Ultra-Trace Amounts of Uranium and Plutonium Using MC-ICP-MS

Mass Spectrometry Letters, (P)2233-4203; (E)2093-8950
2015, v.6 no.3, pp.75-79
https://doi.org/10.5478/MSL.2015.6.3.75
Lim Sang Ho (Korea Atomic Energy Research Institute, University of Science and Technology)
Han Sun-Ho (Korea Atomic Energy Research Institute)
Park Jong-Ho (Korea Atomic Energy Research Institute, University of Science and Technology)
Park Ranhee (Korea Atomic Energy Research Institute)
Lee Min Young (Korea Atomic Energy Research Institute)
Park Jinkyu (Korea Atomic Energy Research Institute)
Lee Chi-Gyu (Korea Atomic Energy Research Institute)
Song Kyuseok (Korea Atomic Energy Research Institute)
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Abstract

Suitable analytical procedures for the bulk analysis of ultra-trace amounts of uranium and plutonium have been developed using multi-collector inductively coupled mass spectrometry (MC–ICP–MS). The quantification and determination of the isotopic ratios of uranium and plutonium in three simulated swipe samples, a swipe blank, and a process blank were per- formed to validate the analytical performance. The analytical results for the simulated swipe samples were in good agreement with the certified values, based on the measurement quality goals for the analysis of bulk environmental samples recommended by the International Atomic Energy Agency (IAEA)

keywords
Bulk analysis Environmental samples Chemical separation IDMS MC-ICP-MS


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Submission Date
2015-08-21
Revised Date
2015-09-04
Accepted Date
2015-09-07
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